Crystallography Open Database

Information card for entry 7123935

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Coordinates	7123935.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C41 H58 Pb
Calculated formula	C41 H58 Pb
Title of publication	Low valent lead hydride chemistry: hydroplumbylation of phenylacetylene and 1,1-dimethylallene
Authors of publication	Wesemann, Lars; Weiß, Sebastian; Schubert, Hartmut
Journal of publication	Chemical Communications
Year of publication	2019
a	14.097 ± 0.0003 Å
b	16.7228 ± 0.0004 Å
c	17.7335 ± 0.0004 Å
α	104.066 ± 0.001°
β	102.058 ± 0.001°
γ	108.956 ± 0.001°
Cell volume	3641.58 ± 0.15 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	3
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0551
Residual factor for significantly intense reflections	0.0389
Weighted residual factors for significantly intense reflections	0.0984
Weighted residual factors for all reflections included in the refinement	0.1072
Goodness-of-fit parameter for all reflections included in the refinement	1.067
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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