Information card for entry 7123949

Structure parameters

• Formula: C100 H92 N9 O8 Rh4 S4
• Calculated formula: C100 H92 N9 O8 Rh4 S4
• Title of publication: Rhodium(I)-Catalyzed Mono-Selective C‒H Alkylation of Benzenesulfonamides with Terminal Alkenes
• Authors of publication: Rej, Supriya; Chatani, Naoto
• Journal of publication: Chemical Communications
• Year of publication: 2019
• a: 11.8864 ± 0.0002 Å
• b: 11.9049 ± 0.00019 Å
• c: 18.32387 ± 0.00016 Å
• α: 96.2059 ± 0.001°
• β: 97.9083 ± 0.0011°
• γ: 115.602 ± 0.0016°
• Cell volume: 2275 ± 0.07 ų
• Cell temperature: 123 K
• Ambient diffraction temperature: 123 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0576
• Residual factor for significantly intense reflections: 0.0558
• Weighted residual factors for significantly intense reflections: 0.1564
• Weighted residual factors for all reflections included in the refinement: 0.1582
• Goodness-of-fit parameter for all reflections included in the refinement: 1.039
• Diffraction radiation wavelength: 1.54187 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No