Information card for entry 7124169

Structure parameters

• Formula: C22 H28 B N2 O4 P
• Calculated formula: C22 H28 B N2 O4 P
• Title of publication: 1,1-Phosphinoboration of Diazomethanes
• Authors of publication: Trofimova, Alina; LaFortune, James; Qu, Zheng-wang; Westcott, Stephen; Stephan, Douglas W.
• Journal of publication: Chemical Communications
• Year of publication: 2019
• a: 13.515 ± 0.0013 Å
• b: 12.4763 ± 0.0013 Å
• c: 13.4773 ± 0.0013 Å
• α: 90°
• β: 97.705 ± 0.004°
• γ: 90°
• Cell volume: 2252 ± 0.4 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150.15 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0456
• Residual factor for significantly intense reflections: 0.035
• Weighted residual factors for significantly intense reflections: 0.0927
• Weighted residual factors for all reflections included in the refinement: 0.1008
• Goodness-of-fit parameter for all reflections included in the refinement: 1.006
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No