Crystallography Open Database

Information card for entry 7124173

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Coordinates	7124173.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C43.5 H43 B Cl N2 P
Calculated formula	C43.5 H43 B Cl N2 P
Title of publication	1,1-Phosphinoboration of Diazomethanes
Authors of publication	Trofimova, Alina; LaFortune, James; Qu, Zheng-wang; Westcott, Stephen; Stephan, Douglas W.
Journal of publication	Chemical Communications
Year of publication	2019
a	11.4929 ± 0.0015 Å
b	12.5079 ± 0.0014 Å
c	13.5474 ± 0.0017 Å
α	95.608 ± 0.006°
β	107.365 ± 0.006°
γ	97.228 ± 0.006°
Cell volume	1825 ± 0.4 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150.15 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1209
Residual factor for significantly intense reflections	0.057
Weighted residual factors for significantly intense reflections	0.1141
Weighted residual factors for all reflections included in the refinement	0.1396
Goodness-of-fit parameter for all reflections included in the refinement	1.0275
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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