Information card for entry 7124226

Structure parameters

• Formula: C33 H33 B F6 N9 O2 P Pt W
• Calculated formula: C33 H33 B F6 N9 O2 P Pt W
• Title of publication: Tungsten-Platinum μ-Carbido and μ-Methylidyne Complexes
• Authors of publication: Hill, Anthony; Frogley, Benjamin
• Journal of publication: Chemical Communications
• Year of publication: 2019
• a: 19.2295 ± 0.0003 Å
• b: 7.9562 ± 0.0002 Å
• c: 27.8172 ± 0.0005 Å
• α: 90°
• β: 100.5 ± 0.002°
• γ: 90°
• Cell volume: 4184.59 ± 0.15 ų
• Cell temperature: 150 ± 0.1 K
• Ambient diffraction temperature: 150 ± 0.1 K
• Number of distinct elements: 9
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0451
• Residual factor for significantly intense reflections: 0.0406
• Weighted residual factors for significantly intense reflections: 0.0992
• Weighted residual factors for all reflections included in the refinement: 0.1026
• Goodness-of-fit parameter for all reflections included in the refinement: 1.064
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No