Information card for entry 7124263

Structure parameters

• Formula: C33 H29 B F12 P Rh
• Calculated formula: C33 H29 B F12 P Rh
• Title of publication: Strong metal-borane interactions in low-valent cyclopentadienyl Rhodium complexes
• Authors of publication: Boudjelel, Maxime; Ladeira, Sonia; Bouhadir, Ghenwa; Bourissou, Didier
• Journal of publication: Chemical Communications
• Year of publication: 2019
• a: 13.0614 ± 0.0009 Å
• b: 12.3133 ± 0.0006 Å
• c: 20.7087 ± 0.0013 Å
• α: 90°
• β: 105.427 ± 0.004°
• γ: 90°
• Cell volume: 3210.6 ± 0.3 ų
• Cell temperature: 193 ± 2 K
• Ambient diffraction temperature: 193 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0853
• Residual factor for significantly intense reflections: 0.0472
• Weighted residual factors for significantly intense reflections: 0.1018
• Weighted residual factors for all reflections included in the refinement: 0.1196
• Goodness-of-fit parameter for all reflections included in the refinement: 1.038
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No