Information card for entry 7124349

Structure parameters

• Formula: C24 H22 N O3 P Pd
• Calculated formula: C24 H22 N O3 P Pd
• Title of publication: Palladium(II)-catalyzed Oxidative C(sp3)‒P Bond Formation via C(sp3)‒H Bond Activation
• Authors of publication: Chen, Lijin; Zhou, Zhenfei; Zhang, Saifei; Li, Xiaoqian; Ma, Xuebing; Dong, Jiaxing
• Journal of publication: Chemical Communications
• Year of publication: 2019
• a: 8.8937 ± 0.0004 Å
• b: 10.7491 ± 0.0004 Å
• c: 12.9531 ± 0.0005 Å
• α: 114.219 ± 0.004°
• β: 99.926 ± 0.003°
• γ: 98.501 ± 0.003°
• Cell volume: 1078.99 ± 0.09 ų
• Cell temperature: 282 ± 3 K
• Ambient diffraction temperature: 282 ± 3 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0503
• Residual factor for significantly intense reflections: 0.0447
• Weighted residual factors for significantly intense reflections: 0.1146
• Weighted residual factors for all reflections included in the refinement: 0.1203
• Goodness-of-fit parameter for all reflections included in the refinement: 1.052
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No