Information card for entry 7124492

Structure parameters

• Formula: C23.33 H29 F6 N2 P Rh
• Calculated formula: C23.33 H29 F6 N2 P Rh
• Title of publication: Multiple binding modes of an unconjugated bis(pyridine) ligand stabilize low-valent [Cp*Rh] complexes.
• Authors of publication: Lionetti, Davide; Day, Victor W.; Lassalle-Kaiser, Benedikt; Blakemore, James D.
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2018
• Journal volume: 54
• Journal issue: 14
• Pages of publication: 1694 - 1697
• a: 10.68 ± 0.0002 Å
• b: 11.8136 ± 0.0003 Å
• c: 11.8896 ± 0.0003 Å
• α: 117.254 ± 0.0017°
• β: 108.438 ± 0.0017°
• γ: 97.3701 ± 0.0017°
• Cell volume: 1196.94 ± 0.06 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 199.99 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0687
• Residual factor for significantly intense reflections: 0.0582
• Weighted residual factors for significantly intense reflections: 0.1448
• Weighted residual factors for all reflections included in the refinement: 0.1534
• Goodness-of-fit parameter for all reflections included in the refinement: 1.065
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No