Information card for entry 7124911

Structure parameters

• Formula: C45 H54 Br N O3 Si Zn
• Calculated formula: C45 H54 Br N O3 Si Zn
• Title of publication: Two-coordinate terminal zinc hydride complexes: synthesis, structure and preliminary reactivity studies.
• Authors of publication: Dawkins, Michael J. C.; Middleton, Ewart; Kefalidis, Christos E.; Dange, Deepak; Juckel, Martin M.; Maron, Laurent; Jones, Cameron
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2016
• Journal volume: 52
• Journal issue: 69
• Pages of publication: 10490 - 10492
• a: 20.9835 ± 0.001 Å
• b: 20.9835 ± 0.001 Å
• c: 37.613 ± 0.003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 16561.3 ± 1.7 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 7
• Space group number: 88
• Hermann-Mauguin space group symbol: I 41/a :2
• Hall space group symbol: -I 4ad
• Residual factor for all reflections: 0.112
• Residual factor for significantly intense reflections: 0.0597
• Weighted residual factors for significantly intense reflections: 0.1136
• Weighted residual factors for all reflections included in the refinement: 0.1364
• Goodness-of-fit parameter for all reflections included in the refinement: 1.023
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No