Information card for entry 7124913

Structure parameters

• Formula: C44 H53 N Si Zn
• Calculated formula: C44 H53 N Si Zn
• Title of publication: Two-coordinate terminal zinc hydride complexes: synthesis, structure and preliminary reactivity studies.
• Authors of publication: Dawkins, Michael J. C.; Middleton, Ewart; Kefalidis, Christos E.; Dange, Deepak; Juckel, Martin M.; Maron, Laurent; Jones, Cameron
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2016
• Journal volume: 52
• Journal issue: 69
• Pages of publication: 10490 - 10492
• a: 18.699 ± 0.004 Å
• b: 10.648 ± 0.002 Å
• c: 37.755 ± 0.008 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 7517 ± 3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.102
• Residual factor for significantly intense reflections: 0.0711
• Weighted residual factors for significantly intense reflections: 0.1865
• Weighted residual factors for all reflections included in the refinement: 0.2061
• Goodness-of-fit parameter for all reflections included in the refinement: 1.06
• Diffraction radiation wavelength: 0.7109 Å
• Diffraction radiation type: Synchrotron
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No