Information card for entry 7125433

Structure parameters

• Formula: C25 H29 B N8 O2 W
• Calculated formula: C25 H29 B N8 O2 W
• Title of publication: Synthesis of pyridyl carbyne complexes and their conversion to N-heterocyclic vinylidenes
• Authors of publication: Hill, Anthony; Frogley, Benjamin
• Journal of publication: Chemical Communications
• Year of publication: 2019
• a: 15.3086 ± 0.0006 Å
• b: 9.8592 ± 0.0004 Å
• c: 17.7914 ± 0.0007 Å
• α: 90°
• β: 96.715 ± 0.004°
• γ: 90°
• Cell volume: 2666.85 ± 0.18 ų
• Cell temperature: 150 ± 0.1 K
• Ambient diffraction temperature: 150 ± 0.1 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0538
• Residual factor for significantly intense reflections: 0.0455
• Weighted residual factors for significantly intense reflections: 0.0833
• Weighted residual factors for all reflections included in the refinement: 0.0865
• Goodness-of-fit parameter for all reflections included in the refinement: 1.163
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No