Information card for entry 7125435

Structure parameters

• Formula: C43 H50 Au2 B2 Cl2 N14 O4 W2
• Calculated formula: C43 H50 Au2 B2 Cl2 N14 O4 W2
• Title of publication: Synthesis of pyridyl carbyne complexes and their conversion to N-heterocyclic vinylidenes
• Authors of publication: Hill, Anthony; Frogley, Benjamin
• Journal of publication: Chemical Communications
• Year of publication: 2019
• a: 12.7628 ± 0.0002 Å
• b: 40.553 ± 0.0005 Å
• c: 11.3383 ± 0.0001 Å
• α: 90°
• β: 91.898 ± 0.001°
• γ: 90°
• Cell volume: 5865.14 ± 0.13 ų
• Cell temperature: 150 ± 0.1 K
• Ambient diffraction temperature: 150 ± 0.1 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0655
• Residual factor for significantly intense reflections: 0.0634
• Weighted residual factors for significantly intense reflections: 0.1353
• Weighted residual factors for all reflections included in the refinement: 0.1363
• Goodness-of-fit parameter for all reflections included in the refinement: 1.18
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No