Information card for entry 7125512

Structure parameters

• Formula: C37 H81 O4 Re Si3
• Calculated formula: C37 H81 O4 Re Si3
• Title of publication: (silox)3RePMe3 (silox = tBu3SiO) is carbonylated to the double insertion product (silox)(Me3P){cis-(CO)2}Re{ trans-(CO2SitBu3)2 }
• Authors of publication: Veige, Adam S.; Wolczanski, Peter T.; Lobkovsky, Emil B.
• Journal of publication: Chemical Communications
• Year of publication: 2001
• Journal issue: 24
• Pages of publication: 2734
• a: 8.701 ± 0.0017 Å
• b: 21.072 ± 0.004 Å
• c: 24.334 ± 0.005 Å
• α: 90°
• β: 93.89 ± 0.03°
• γ: 90°
• Cell volume: 4451.3 ± 1.5 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0956
• Residual factor for significantly intense reflections: 0.0896
• Weighted residual factors for significantly intense reflections: 0.2227
• Weighted residual factors for all reflections included in the refinement: 0.2278
• Goodness-of-fit parameter for all reflections included in the refinement: 1.015
• Diffraction radiation wavelength: 0.94862 Å
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No