Information card for entry 7125715

Structure parameters

• Chemical name: Amol
• Formula: C22 H28 N2 O2
• Calculated formula: C22 H28 N2 O2
• Title of publication: para-Selective copper-catalyzed C(sp²)-H amidation/dimerization of anilides via a radical pathway.
• Authors of publication: Viveki, Amol B.; Garad, Dnyaneshwar N.; Gonnade, Rajesh G.; Mhaske, Santosh B.
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2020
• Journal volume: 56
• Journal issue: 10
• Pages of publication: 1565 - 1568
• a: 18.3781 ± 0.0007 Å
• b: 9.6218 ± 0.0004 Å
• c: 11.0075 ± 0.0004 Å
• α: 90°
• β: 101.862 ± 0.002°
• γ: 90°
• Cell volume: 1904.9 ± 0.13 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0715
• Residual factor for significantly intense reflections: 0.0473
• Weighted residual factors for significantly intense reflections: 0.0965
• Weighted residual factors for all reflections included in the refinement: 0.1065
• Goodness-of-fit parameter for all reflections included in the refinement: 1.018
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No