Modular synthesis of (C-10 to C-13)-substituted-9,14-diaryl-9,14-dihydrodibenzo[a,c]phenazines via a subsequent Buchwald-Hartwig amination and C-H amination strategy.
Authors of publication
Li, Xiaobin; Zhang, Chengxi; Wang, Chenchen; Ye, Wenqiang; Zhang, Qian; Zhang, Zhiyun; Su, Jianhua; Chen, Yifeng; Tian, He
Journal of publication
Chemical communications (Cambridge, England)
Year of publication
2020
Journal volume
56
Journal issue
15
Pages of publication
2260 - 2263
a
7.9242 ± 0.0003 Å
b
9.1825 ± 0.0004 Å
c
18.631 ± 0.0008 Å
α
90°
β
93 ± 0.001°
γ
90°
Cell volume
1353.81 ± 0.1 Å3
Cell temperature
293 ± 2 K
Ambient diffraction temperature
293 ± 2 K
Number of distinct elements
4
Space group number
7
Hermann-Mauguin space group symbol
P 1 n 1
Hall space group symbol
P -2yac
Residual factor for all reflections
0.0422
Residual factor for significantly intense reflections
0.0355
Weighted residual factors for significantly intense reflections
0.0827
Weighted residual factors for all reflections included in the refinement
0.0877
Goodness-of-fit parameter for all reflections included in the refinement
