Information card for entry 7126254

Structure parameters

• Chemical name: Tetrakis(bis(1,2,3,4-tetra(isopropyl)cyclopentadienyl)-azido-uranium(iii)) n-pentane solvate
• Formula: C141 H244 N12 U4
• Calculated formula: C141 H244 N12 U4
• Title of publication: Lewis acid capping of a uranium(v) nitride via a uranium(iii) azide molecular square.
• Authors of publication: Boreen, Michael A.; Rao, Guodong; Villarreal, David G.; Watt, Fabian A.; Britt, R. David; Hohloch, Stephan; Arnold, John
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2020
• Journal volume: 56
• Journal issue: 33
• Pages of publication: 4535 - 4538
• a: 20.7855 ± 0.0005 Å
• b: 20.7855 ± 0.0005 Å
• c: 35.3744 ± 0.001 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 15283.1 ± 0.7 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 4
• Space group number: 94
• Hermann-Mauguin space group symbol: P 42 21 2
• Hall space group symbol: P 4n 2n
• Residual factor for all reflections: 0.0501
• Residual factor for significantly intense reflections: 0.0356
• Weighted residual factors for significantly intense reflections: 0.067
• Weighted residual factors for all reflections included in the refinement: 0.0712
• Goodness-of-fit parameter for all reflections included in the refinement: 1.03
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No