Information card for entry 7126371

Structure parameters

• Formula: C26 H35 B O3
• Calculated formula: C26 H35 B O3
• Title of publication: Consecutive borylcupration/C-C coupling of γ-alkenyl aldehydes towards diastereoselective 2-(borylmethyl)cycloalkanols.
• Authors of publication: Maza, Ricardo J.; Royes, Jordi; Carbó, Jorge J; Fernández, Elena
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2020
• Journal volume: 56
• Journal issue: 44
• Pages of publication: 5973 - 5976
• a: 17.9052 ± 0.0016 Å
• b: 6.4987 ± 0.0006 Å
• c: 19.8249 ± 0.0016 Å
• α: 90°
• β: 100.138 ± 0.003°
• γ: 90°
• Cell volume: 2270.8 ± 0.3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1147
• Residual factor for significantly intense reflections: 0.0663
• Weighted residual factors for significantly intense reflections: 0.1626
• Weighted residual factors for all reflections included in the refinement: 0.1886
• Goodness-of-fit parameter for all reflections included in the refinement: 1.025
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No