Information card for entry 7126982

Structure parameters

• Formula: H129 La9 O240 Si3 W44
• Calculated formula: La9 O204 Si3 W44.0004
• Title of publication: All-inorganic open frameworks based on gigantic four-shell Ln@W₈@Ln₈@(SiW₁₂)₆ clusters.
• Authors of publication: Liu, Jin-Hua; Lin, Li-Dan; Wang, Guo-Qiang; Li, Ling-Yun; Sun, Yan-Qiong; Li, Xin-Xiong; Zheng, Shou-Tian
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2020
• Journal volume: 56
• Journal issue: 71
• Pages of publication: 10305 - 10308
• a: 37.5612 ± 0.0003 Å
• b: 37.5612 ± 0.0003 Å
• c: 37.5612 ± 0.0003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 52993 ± 0.7 ų
• Cell temperature: 175 ± 2 K
• Ambient diffraction temperature: 175 ± 2 K
• Number of distinct elements: 5
• Space group number: 226
• Hermann-Mauguin space group symbol: F m -3 c
• Hall space group symbol: -F 4a 2 3
• Residual factor for all reflections: 0.0346
• Residual factor for significantly intense reflections: 0.0319
• Weighted residual factors for significantly intense reflections: 0.09
• Weighted residual factors for all reflections included in the refinement: 0.0916
• Goodness-of-fit parameter for all reflections included in the refinement: 1.099
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No