Information card for entry 7126996

Structure parameters

• Formula: C35 H37 Cl6.39 N5 O2 Ru Sb
• Calculated formula: C35 H37 Cl6.3902 N5 O2 Ru Sb
• Title of publication: A metastable Ru^III azido complex with metallo-Staudinger reactivity.
• Authors of publication: Park, Sungho V.; Fry, Charles G.; Bill, Eckhard; Berry, John F.
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2020
• Journal volume: 56
• Journal issue: 73
• Pages of publication: 10738 - 10741
• a: 23.348 ± 0.007 Å
• b: 13.355 ± 0.004 Å
• c: 12.292 ± 0.004 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 3833 ± 2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 7
• Space group number: 62
• Hermann-Mauguin space group symbol: P n m a
• Hall space group symbol: -P 2ac 2n
• Residual factor for all reflections: 0.048
• Residual factor for significantly intense reflections: 0.041
• Weighted residual factors for significantly intense reflections: 0.0919
• Weighted residual factors for all reflections included in the refinement: 0.0955
• Goodness-of-fit parameter for all reflections included in the refinement: 1.159
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No