Information card for entry 7127013

Structure parameters

• Common name: LSnFeNNSiMe3(3),18198
• Formula: C88 H148 Fe2 N12 O P6 Si2 Sn2
• Calculated formula: C88 H148 Fe2 N12 O P6 Si2 Sn2
• Title of publication: Bimetallic iron-tin catalyst for N₂ to NH₃ and a silyldiazenido model intermediate.
• Authors of publication: Dorantes, Michael J.; Moore, James T.; Bill, Eckhard; Mienert, Bernd; Lu, Connie C.
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2020
• Journal volume: 56
• Journal issue: 75
• Pages of publication: 11030 - 11033
• a: 11.4678 ± 0.0013 Å
• b: 21.538 ± 0.002 Å
• c: 19.703 ± 0.002 Å
• α: 90°
• β: 96.834 ± 0.004°
• γ: 90°
• Cell volume: 4831.9 ± 0.9 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0697
• Residual factor for significantly intense reflections: 0.0442
• Weighted residual factors for significantly intense reflections: 0.074
• Weighted residual factors for all reflections included in the refinement: 0.0812
• Goodness-of-fit parameter for all reflections included in the refinement: 1.055
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No