Information card for entry 7127385

Structure parameters

• Formula: C11.89 H31.67 Cl0.11 Li3 N3
• Calculated formula: C11.889 H31.667 Cl0.111 Li3 N3
• Title of publication: The structure-defining incorporation of chloride in methyllithium dimers.
• Authors of publication: Knauer, Lena; Strohmann, Carsten
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2020
• Journal volume: 56
• Journal issue: 88
• Pages of publication: 13543 - 13546
• a: 19.9942 ± 0.0006 Å
• b: 11.0399 ± 0.0003 Å
• c: 17.1245 ± 0.0005 Å
• α: 90°
• β: 110.506 ± 0.001°
• γ: 90°
• Cell volume: 3540.44 ± 0.18 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 99.99 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0517
• Residual factor for significantly intense reflections: 0.0424
• Weighted residual factors for significantly intense reflections: 0.1108
• Weighted residual factors for all reflections included in the refinement: 0.1175
• Goodness-of-fit parameter for all reflections included in the refinement: 1.042
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No