Information card for entry 7127409

Structure parameters

• Formula: C35 H61 Li O6 P4 Ta
• Calculated formula: C35 H61 Li O6 P4 Ta
• Title of publication: The reaction behavior of [Cp₂Mo₂(CO)₄(μ,η^2:2-P₂)] and [Cp''Ta(CO)₂(η⁴-P₄)] towards hydroxide and tert-butyl nucleophiles.
• Authors of publication: Riedlberger, Felix; Seidl, Michael; Scheer, Manfred
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2020
• Journal volume: 56
• Journal issue: 89
• Pages of publication: 13836 - 13839
• a: 11.8625 ± 0.0001 Å
• b: 21.7618 ± 0.0003 Å
• c: 16.0909 ± 0.0002 Å
• α: 90°
• β: 94.017 ± 0.001°
• γ: 90°
• Cell volume: 4143.65 ± 0.08 ų
• Cell temperature: 123 ± 0.1 K
• Ambient diffraction temperature: 123 ± 0.1 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0542
• Residual factor for significantly intense reflections: 0.0503
• Weighted residual factors for significantly intense reflections: 0.1318
• Weighted residual factors for all reflections included in the refinement: 0.1366
• Goodness-of-fit parameter for all reflections included in the refinement: 1.031
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No