Information card for entry 7127467

Structure parameters

• Formula: C24 H132 Cs7.5 Dy4 K0.5 O180 P8 W32
• Calculated formula: C21.48 H17.48 Cs7.4722 Dy4 K0.5 O161 P8 W32
• Title of publication: Polyoxometalates with separate lacuna sites.
• Authors of publication: Wang, Wenyan; Izarova, Natalya V.; van Leusen, Jan; Kögerler, Paul
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2020
• Journal volume: 56
• Journal issue: 94
• Pages of publication: 14857 - 14860
• a: 12.757 ± 0.003 Å
• b: 14.616 ± 0.003 Å
• c: 24.915 ± 0.005 Å
• α: 73.84 ± 0.03°
• β: 86.54 ± 0.03°
• γ: 79.7 ± 0.03°
• Cell volume: 4389.8 ± 1.8 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1357
• Residual factor for significantly intense reflections: 0.087
• Weighted residual factors for significantly intense reflections: 0.2206
• Weighted residual factors for all reflections included in the refinement: 0.2469
• Goodness-of-fit parameter for all reflections included in the refinement: 0.994
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No