Information card for entry 7127772

Structure parameters

• Formula: C32 H42 Cl8 Ni2 O14 P2
• Calculated formula: C32 H42 Cl8 Ni2 O14 P2
• Title of publication: Oxyphosphoranes as precursors to bridging phosphate-catecholate ligands.
• Authors of publication: Yang, Xin; Wei, Rui; Shi, Yaping; Liu, Liu Leo; Wu, Yile; Zhao, Yufen; Stephan, Douglas W.
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2021
• Journal volume: 57
• Journal issue: 10
• Pages of publication: 1194 - 1197
• a: 8.911 ± 0.0005 Å
• b: 11.1675 ± 0.0006 Å
• c: 11.8597 ± 0.0007 Å
• α: 108.483 ± 0.0015°
• β: 97.6582 ± 0.0016°
• γ: 100.322 ± 0.0015°
• Cell volume: 1078.12 ± 0.11 ų
• Cell temperature: 103 ± 2 K
• Ambient diffraction temperature: 103 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0329
• Residual factor for significantly intense reflections: 0.0325
• Weighted residual factors for significantly intense reflections: 0.0853
• Weighted residual factors for all reflections included in the refinement: 0.0856
• Goodness-of-fit parameter for all reflections included in the refinement: 1.06
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No