Information card for entry 7127775

Structure parameters

• Formula: C40 H58 Cl10 O16 P2 V2
• Calculated formula: C40 H58 Cl10 O16 P2 V2
• Title of publication: Oxyphosphoranes as precursors to bridging phosphate-catecholate ligands.
• Authors of publication: Yang, Xin; Wei, Rui; Shi, Yaping; Liu, Liu Leo; Wu, Yile; Zhao, Yufen; Stephan, Douglas W.
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2021
• Journal volume: 57
• Journal issue: 10
• Pages of publication: 1194 - 1197
• a: 14.4834 ± 0.0009 Å
• b: 14.9881 ± 0.0009 Å
• c: 15.571 ± 0.001 Å
• α: 107.35 ± 0.002°
• β: 117.247 ± 0.002°
• γ: 98.551 ± 0.002°
• Cell volume: 2701.5 ± 0.3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0438
• Residual factor for significantly intense reflections: 0.0424
• Weighted residual factors for significantly intense reflections: 0.1157
• Weighted residual factors for all reflections included in the refinement: 0.1174
• Goodness-of-fit parameter for all reflections included in the refinement: 1.044
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No