Information card for entry 7127956

Structure parameters

• Formula: C48 H54 N0 Ni3 S6
• Calculated formula: C48 H54 Ni3 S6
• Title of publication: Reversible polymorphic structural transition of crown-like nickel nanoclusters and its effect on conductivity.
• Authors of publication: Maman, Manju P.; Nath, Akashdeep; Anjusree S, ?; Das, Bikas C.; Mandal, Sukhendu
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2021
• Journal volume: 57
• Journal issue: 23
• Pages of publication: 2935 - 2938
• a: 11.329 ± 0.005 Å
• b: 12.521 ± 0.006 Å
• c: 32.774 ± 0.015 Å
• α: 90°
• β: 91.641 ± 0.005°
• γ: 90°
• Cell volume: 4647 ± 4 ų
• Cell temperature: 298 ± 2 K
• Ambient diffraction temperature: 298 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1924
• Residual factor for significantly intense reflections: 0.1093
• Weighted residual factors for significantly intense reflections: 0.2651
• Weighted residual factors for all reflections included in the refinement: 0.3115
• Goodness-of-fit parameter for all reflections included in the refinement: 1.167
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No