Information card for entry 7128321

Structure parameters

• Chemical name: catena-[bis(m-hydroxo)-bis(m-oxo)-tris(m-terephthalato)-tri-Thulium]
• Formula: C24 H12 O16 Tm3
• Calculated formula: C24 H12 O16 Tm3
• Title of publication: Synthetic approaches for accessing rare-earth analogues of UiO-66.
• Authors of publication: Donnarumma, P. Rafael; Frojmovic, Sahara; Marino, Paola; Bicalho, Hudson A.; Titi, Hatem M.; Howarth, Ashlee J.
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2021
• Journal volume: 57
• Journal issue: 50
• Pages of publication: 6121 - 6124
• a: 21.2553 ± 0.0016 Å
• b: 21.2553 ± 0.0016 Å
• c: 21.2553 ± 0.0016 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 9602.9 ± 1.3 ų
• Cell temperature: 253 ± 2 K
• Ambient diffraction temperature: 253 ± 2 K
• Number of distinct elements: 4
• Space group number: 225
• Hermann-Mauguin space group symbol: F m -3 m
• Hall space group symbol: -F 4 2 3
• Residual factor for all reflections: 0.0433
• Residual factor for significantly intense reflections: 0.0369
• Weighted residual factors for significantly intense reflections: 0.095
• Weighted residual factors for all reflections included in the refinement: 0.1065
• Goodness-of-fit parameter for all reflections included in the refinement: 1.091
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No