Information card for entry 7128381

Structure parameters

• Formula: C20 H33 B O5 Si
• Calculated formula: C20 H33 B O5 Si
• SMILES: [Si](/C(=C/c1c(OC)cc(OC)cc1OC)B1OC(C)(C)C(O1)(C)C)(C)(C)C
• Title of publication: A modular olefination reaction between aldehydes and diborylsilylmethide lithium salts.
• Authors of publication: Salvado, Oriol; Fernández, Elena
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2021
• Journal volume: 57
• Journal issue: 51
• Pages of publication: 6300 - 6303
• a: 7.32916 ± 0.00012 Å
• b: 16.4248 ± 0.0002 Å
• c: 18.857 ± 0.0003 Å
• α: 90°
• β: 100.201 ± 0.0016°
• γ: 90°
• Cell volume: 2234.12 ± 0.06 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.033
• Residual factor for significantly intense reflections: 0.0298
• Weighted residual factors for significantly intense reflections: 0.0884
• Weighted residual factors for all reflections included in the refinement: 0.0903
• Goodness-of-fit parameter for all reflections included in the refinement: 1.045
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No