Information card for entry 7128495

Structure parameters

• Formula: C62 H58 N4 Si2
• Calculated formula: C2.48 H2.32 N0.16 Si0.08
• Title of publication: Facile synthesis of tribenzosilepins from terphenyls and dihydrosilanes by electrophilic double silylation.
• Authors of publication: Dong, Yafang; Sekine, Kohei; Kuninobu, Yoichiro
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2021
• Journal volume: 57
• Journal issue: 57
• Pages of publication: 7007 - 7010
• a: 15.3334 ± 0.0008 Å
• b: 11.1613 ± 0.0008 Å
• c: 15.7358 ± 0.0009 Å
• α: 90°
• β: 91.89 ± 0.005°
• γ: 90°
• Cell volume: 2691.6 ± 0.3 ų
• Cell temperature: 173 K
• Ambient diffraction temperature: 173 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0791
• Residual factor for significantly intense reflections: 0.0615
• Weighted residual factors for significantly intense reflections: 0.1631
• Weighted residual factors for all reflections included in the refinement: 0.172
• Goodness-of-fit parameter for all reflections included in the refinement: 1.052
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No