Information card for entry 7128568

Structure parameters

• Formula: C21 H29 N Si
• Calculated formula: C21 H29 N Si
• Title of publication: Direct formation of 4,5-disubstituted carbazoles via regioselective dilithiation.
• Authors of publication: Pocock, Ian A.; Alotaibi, Alya M.; Jagdev, Kesar; Prior, Connor; Burgess, Gregory R.; Male, Louise; Grainger, Richard S.
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2021
• Journal volume: 57
• Journal issue: 59
• Pages of publication: 7252 - 7255
• a: 9.3498 ± 0.0004 Å
• b: 7.3678 ± 0.0003 Å
• c: 27.1186 ± 0.001 Å
• α: 90°
• β: 98.469 ± 0.004°
• γ: 90°
• Cell volume: 1847.76 ± 0.13 ų
• Cell temperature: 100.01 ± 0.1 K
• Ambient diffraction temperature: 100.01 ± 0.1 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0679
• Residual factor for significantly intense reflections: 0.0581
• Weighted residual factors for significantly intense reflections: 0.1456
• Weighted residual factors for all reflections included in the refinement: 0.1522
• Goodness-of-fit parameter for all reflections included in the refinement: 1.052
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No