Crystallography Open Database

Information card for entry 7128618

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Coordinates	7128618.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	H48 N12 O78 Sb8 V30
Calculated formula	H32 N12 O78 Sb8 V30
Title of publication	Three intersecting {V<sub>12</sub>} rings: {V<sub>30</sub>Sb<sub>8</sub>}, an ultra-large polyoxovanadate cluster shell.
Authors of publication	Lühmann, Henning; Näther, Christian; van Leusen, Jan; Kögerler, Paul; Bensch, Wolfgang
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2021
Journal volume	57
Journal issue	62
Pages of publication	7661 - 7664
a	16.2776 ± 0.0007 Å
b	16.2776 ± 0.0007 Å
c	17.752 ± 0.0009 Å
α	90°
β	90°
γ	90°
Cell volume	4703.6 ± 0.4 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	5
Space group number	87
Hermann-Mauguin space group symbol	I 4/m
Hall space group symbol	-I 4
Residual factor for all reflections	0.0618
Residual factor for significantly intense reflections	0.0415
Weighted residual factors for significantly intense reflections	0.0991
Weighted residual factors for all reflections included in the refinement	0.1072
Goodness-of-fit parameter for all reflections included in the refinement	1.034
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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