Information card for entry 7128747

Structure parameters

• Formula: C18 H40 Al F20 O4 P Si4 Te4
• Calculated formula: C18 H40 Al F20 O4 P Si4 Te4
• SMILES: [Te](F)(F)(F)(F)(F)O[Al](O[Te](F)(F)(F)(F)F)(O[Te](F)(F)(F)(F)F)O[Te](F)(F)(F)(F)F.[p+]1(c([Si](C)(C)C)c(cc(c1[Si](C)(C)C)[Si](C)(C)C)[Si](C)(C)C)C
• Title of publication: One-step methylation of aromatic phosphorus heterocycles: synthesis and crystallographic characterization of a 1-methyl-phosphininium salt.
• Authors of publication: Fischer, Lukas; Wossidlo, Friedrich; Frost, Daniel; Coles, Nathan T.; Steinhauer, Simon; Riedel, Sebastian; Müller, Christian
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2021
• Journal volume: 57
• Journal issue: 75
• Pages of publication: 9522 - 9525
• a: 12.0027 ± 0.0004 Å
• b: 16.9978 ± 0.0005 Å
• c: 21.5539 ± 0.0007 Å
• α: 90°
• β: 90.59 ± 0.001°
• γ: 90°
• Cell volume: 4397.2 ± 0.2 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 8
• Space group number: 9
• Hermann-Mauguin space group symbol: C 1 c 1
• Hall space group symbol: C -2yc
• Residual factor for all reflections: 0.018
• Residual factor for significantly intense reflections: 0.0174
• Weighted residual factors for significantly intense reflections: 0.0416
• Weighted residual factors for all reflections included in the refinement: 0.0421
• Goodness-of-fit parameter for all reflections included in the refinement: 1.048
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No