Information card for entry 7128856

Structure parameters

• Formula: C71 H63 B2 F8 Pd2 Pt4
• Calculated formula: C71 H63 B2 F8 Pd2 Pt4
• Title of publication: Selective dimerization of a trinuclear mixed-metal sandwich complex: construction of an axially chiral metal skeleton.
• Authors of publication: Yamaura, Hiroshige; Yamamoto, Koji; Murahashi, Tetsuro
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2021
• Journal volume: 57
• Journal issue: 72
• Pages of publication: 9120 - 9123
• a: 12.7384 ± 0.0003 Å
• b: 15.0444 ± 0.0004 Å
• c: 16.389 ± 0.0004 Å
• α: 89.1192 ± 0.0007°
• β: 80.0982 ± 0.0007°
• γ: 75.3532 ± 0.0007°
• Cell volume: 2992.18 ± 0.13 ų
• Cell temperature: 123 K
• Ambient diffraction temperature: 123 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0291
• Residual factor for significantly intense reflections: 0.0257
• Weighted residual factors for significantly intense reflections: 0.0629
• Weighted residual factors for all reflections included in the refinement: 0.0643
• Goodness-of-fit parameter for all reflections included in the refinement: 1.042
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No