Information card for entry 7129977

Structure parameters

• Formula: C98 H70 B Cr2 F24 O6 P2 Rh
• Calculated formula: C98 H70 B Cr2 F24 O6 P2 Rh
• Title of publication: Highly Flexible Phosphabenzenes: A Missing Coordination Mode of 2,4,6-Triaryl-λ3-Phosphinines
• Authors of publication: Yue, Erlin; Petrov, Andrey; Frost, Daniel Sebastian; Dettling, Lea; Conrad, Lawrence; Wossidlo, Friedrich; Coles, Nathan Thomas; Weber, Manuela; Muller, Christian
• Journal of publication: Chemical Communications
• Year of publication: 2022
• a: 10.25337 ± 0.00007 Å
• b: 32.9923 ± 0.0002 Å
• c: 29.7568 ± 0.0002 Å
• α: 90°
• β: 92.1304 ± 0.0004°
• γ: 90°
• Cell volume: 10059.2 ± 0.11 ų
• Cell temperature: 102.6 K
• Ambient diffraction temperature: 102.6 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1049
• Residual factor for significantly intense reflections: 0.0951
• Weighted residual factors for significantly intense reflections: 0.2193
• Weighted residual factors for all reflections included in the refinement: 0.2246
• Goodness-of-fit parameter for all reflections included in the refinement: 1.099
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No