Information card for entry 7130717

Structure parameters

• Formula: C155 H260 N18 Na10 O143 P16 V26 W6
• Calculated formula: C112 H108 N4 Na10 O128 P16 V26 W6
• Title of publication: High-nuclear polyoxovanadates assembled from pentagonal building blocks
• Authors of publication: Zhang, Ting; Hou, Yuhan; Hou, Baoshan; Zhao, Liang; Wang, Xinlong; Qin, Chao; Su, Zhongmin
• Journal of publication: Chemical Communications
• Year of publication: 2022
• a: 16.228 ± 0.0007 Å
• b: 23.1623 ± 0.0009 Å
• c: 36.289 ± 0.0014 Å
• α: 90°
• β: 92.039 ± 0.002°
• γ: 90°
• Cell volume: 13631.6 ± 1 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173.02 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0869
• Residual factor for significantly intense reflections: 0.0713
• Weighted residual factors for significantly intense reflections: 0.1757
• Weighted residual factors for all reflections included in the refinement: 0.1847
• Goodness-of-fit parameter for all reflections included in the refinement: 1.035
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Diffraction radiation X-ray symbol: K-L~3~
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No