Crystallography Open Database

Information card for entry 7130861

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Coordinates	7130861.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C32 H40 B2 O4 Si
Calculated formula	C32 H40 B2 O4 Si
Title of publication	Directed <i>cis</i>-hydrosilylation of borylalkynes to borylsilylalkenes.
Authors of publication	Stefanowska, Kinga; Sokolnicki, Tomasz; Walkowiak, Jędrzej; Czapik, Agnieszka; Franczyk, Adrian
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2022
Journal volume	58
Journal issue	86
Pages of publication	12046 - 12049
a	10.11404 ± 0.00009 Å
b	16.90606 ± 0.00014 Å
c	18.29331 ± 0.00016 Å
α	90°
β	102.387 ± 0.0009°
γ	90°
Cell volume	3055.13 ± 0.05 Å³
Cell temperature	130 ± 2 K
Ambient diffraction temperature	130 ± 2 K
Number of distinct elements	5
Space group number	9
Hermann-Mauguin space group symbol	C 1 c 1
Hall space group symbol	C -2yc
Residual factor for all reflections	0.0274
Residual factor for significantly intense reflections	0.0273
Weighted residual factors for significantly intense reflections	0.0761
Weighted residual factors for all reflections included in the refinement	0.0762
Goodness-of-fit parameter for all reflections included in the refinement	1.077
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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