Crystallography Open Database

Information card for entry 7130864

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Coordinates	7130864.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C26 H29 B O2 Si
Calculated formula	C26 H29 B1.00168 O2 Si
Title of publication	Directed <i>cis</i>-hydrosilylation of borylalkynes to borylsilylalkenes.
Authors of publication	Stefanowska, Kinga; Sokolnicki, Tomasz; Walkowiak, Jędrzej; Czapik, Agnieszka; Franczyk, Adrian
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2022
Journal volume	58
Journal issue	86
Pages of publication	12046 - 12049
a	19.7542 ± 0.0004 Å
b	20.3725 ± 0.0003 Å
c	21.9182 ± 0.0005 Å
α	96.7187 ± 0.0014°
β	112.361 ± 0.0019°
γ	114.97 ± 0.0017°
Cell volume	6977.9 ± 0.3 Å³
Cell temperature	130 ± 2 K
Ambient diffraction temperature	130 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0564
Residual factor for significantly intense reflections	0.0436
Weighted residual factors for significantly intense reflections	0.1296
Weighted residual factors for all reflections included in the refinement	0.143
Goodness-of-fit parameter for all reflections included in the refinement	1.07
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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