Information card for entry 7131250

Structure parameters

• Formula: C20 H60 Cl4 Ge4 Si10
• Calculated formula: C20 H60 Cl4 Ge4 Si10
• Title of publication: Group IV heteroadamantanes: synthesis of Si₆Sn₄ and site-selective derivatization of Si₆Ge₄.
• Authors of publication: Köstler, Benedikt; Gilmer, Jannik; Bolte, Michael; Virovets, Alexander; Lerner, Hans-Wolfram; Albert, Philipp; Fantuzzi, Felipe; Wagner, Matthias
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2023
• Journal volume: 59
• Journal issue: 16
• Pages of publication: 2295 - 2298
• a: 20.2374 ± 0.0004 Å
• b: 12.5486 ± 0.0003 Å
• c: 37.1944 ± 0.0009 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 9445.6 ± 0.4 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.0909
• Residual factor for significantly intense reflections: 0.0525
• Weighted residual factors for significantly intense reflections: 0.1076
• Weighted residual factors for all reflections included in the refinement: 0.1208
• Goodness-of-fit parameter for all reflections included in the refinement: 1.06
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No