Information card for entry 7131265

Structure parameters

• Formula: C46 H82 Al K N4 O7 Si2
• Calculated formula: C46 H82 Al K N4 O7 Si2
• Title of publication: Reduction chemistry yields stable and soluble divalent lanthanide tris(pyrazolyl)borate complexes.
• Authors of publication: Chowdhury, Tajrian; Evans, Matthew J.; Coles, Martyn P.; Bailey, Anna G.; Peveler, William J.; Wilson, Claire; Farnaby, Joy H.
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2023
• Journal volume: 59
• Journal issue: 15
• Pages of publication: 2134 - 2137
• a: 19.1041 ± 0.0015 Å
• b: 16.1012 ± 0.0015 Å
• c: 19.415 ± 0.002 Å
• α: 90°
• β: 116.588 ± 0.003°
• γ: 90°
• Cell volume: 5340.5 ± 0.9 ų
• Cell temperature: 150 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0694
• Residual factor for significantly intense reflections: 0.0575
• Weighted residual factors for significantly intense reflections: 0.1524
• Weighted residual factors for all reflections included in the refinement: 0.1599
• Goodness-of-fit parameter for all reflections included in the refinement: 1.1
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No