Information card for entry 7131400

Structure parameters

• Formula: C105 H53 F52 N4 O1.5 Sn Tc
• Calculated formula: C105 H53 F52 N4 O1.5 Sn Tc
• Title of publication: Na[Tc(CO)(CN<i>p</i>-F-Ar^DArF2)₄]: an isocyanide analogue of the elusive Na[Tc(CO)₅].
• Authors of publication: Salsi, Federico; Hagenbach, Adelheid; Figueroa, Joshua S.; Abram, Ulrich
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2023
• Journal volume: 59
• Journal issue: 27
• Pages of publication: 4028 - 4031
• a: 14.727 ± 0.005 Å
• b: 15.583 ± 0.009 Å
• c: 50.04 ± 0.03 Å
• α: 94.762 ± 0.007°
• β: 96.185 ± 0.01°
• γ: 94.402 ± 0.012°
• Cell volume: 11335 ± 10 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1403
• Residual factor for significantly intense reflections: 0.1
• Weighted residual factors for significantly intense reflections: 0.2248
• Weighted residual factors for all reflections included in the refinement: 0.245
• Goodness-of-fit parameter for all reflections included in the refinement: 1.05
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No