Information card for entry 7131453

Structure parameters

• Formula: C92 H32 Al4 F144 Fe2 O16
• Calculated formula: C92 H32 Al4 F144 Fe2 O16
• Title of publication: Teaching old tricks to new dogs - rational synthesis of multi-decker complexes featuring <i>cyclo</i>-P₅ decks.
• Authors of publication: Riesinger, Christoph; Röhner, David; Krossing, Ingo; Scheer, Manfred
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2023
• Journal volume: 59
• Journal issue: 30
• Pages of publication: 4495 - 4498
• a: 15.9325 ± 0.0004 Å
• b: 16.1088 ± 0.0004 Å
• c: 26.3304 ± 0.0006 Å
• α: 92.872 ± 0.002°
• β: 91.023 ± 0.002°
• γ: 94.758 ± 0.002°
• Cell volume: 6724.4 ± 0.3 ų
• Cell temperature: 123 ± 0.1 K
• Ambient diffraction temperature: 123 ± 0.1 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0795
• Residual factor for significantly intense reflections: 0.0579
• Weighted residual factors for significantly intense reflections: 0.154
• Weighted residual factors for all reflections included in the refinement: 0.1642
• Goodness-of-fit parameter for all reflections included in the refinement: 0.997
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No