Information card for entry 7131634

Structure parameters

• Formula: C104 H92 N4 O8 S4 Zn4
• Calculated formula: C104 H92 N4 O8 S4 Zn4
• Title of publication: Atom-efficient arylation of <i>N</i>-tosylimines mediated by cooperative ZnAr₂/Zn(C₆F₅)₂ combinations.
• Authors of publication: Borys, Andryj M.; Kunzmann, Tim; Gil-Negrete, Jose M; Hevia, Eva
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2023
• Journal volume: 59
• Journal issue: 49
• Pages of publication: 7583 - 7586
• a: 13.5602 ± 0.0003 Å
• b: 13.8377 ± 0.0003 Å
• c: 14.8499 ± 0.0002 Å
• α: 70.109 ± 0.002°
• β: 81.732 ± 0.002°
• γ: 72.621 ± 0.002°
• Cell volume: 2497.85 ± 0.09 ų
• Cell temperature: 173 ± 0.1 K
• Ambient diffraction temperature: 173 ± 0.1 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.057
• Residual factor for significantly intense reflections: 0.0531
• Weighted residual factors for significantly intense reflections: 0.1477
• Weighted residual factors for all reflections included in the refinement: 0.1506
• Goodness-of-fit parameter for all reflections included in the refinement: 1.071
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No