Information card for entry 7131907

Structure parameters

• Formula: C64 H91 N2 P3 Si
• Calculated formula: C64 H91 N2 P3 Si
• Title of publication: SiP-heterocycles derived from a bulky phosphanylsilylene
• Authors of publication: Li, Yan; Wang, Chenfeng; Su, Ming-Der; Fang, Zijie; Zhou, Jiahao; Zhang, Haoqi; Li, Xiaodi; Zuo, Darui; Zhang, Zheng-Feng
• Journal of publication: Chemical Communications
• Year of publication: 2023
• a: 12.369 ± 0.003 Å
• b: 23.579 ± 0.005 Å
• c: 19.827 ± 0.005 Å
• α: 90°
• β: 98.041 ± 0.009°
• γ: 90°
• Cell volume: 5726 ± 2 ų
• Cell temperature: 170 ± 2 K
• Ambient diffraction temperature: 170 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0886
• Residual factor for significantly intense reflections: 0.0702
• Weighted residual factors for significantly intense reflections: 0.1728
• Weighted residual factors for all reflections included in the refinement: 0.186
• Goodness-of-fit parameter for all reflections included in the refinement: 1.056
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No