Information card for entry 7131945
| Formula |
C27 H23 N3 |
| Calculated formula |
C27 H23 N3 |
| Title of publication |
Accessing indole-isoindole derivatives via palladium-catalyzed [3+2] cyclization of isocyanides with alkynyl imines |
| Authors of publication |
Chen, Dianpeng; Li, Jianming; Liu, Gongle; Zhang, Xiuhua; Wang, Xin; Liu, Yongwei; Liu, Xuan; Liu, Xinghai; Li, Yongqin; Shan, Yingying |
| Journal of publication |
Chemical Communications |
| Year of publication |
2023 |
| a |
10.975 ± 0.0007 Å |
| b |
12.9016 ± 0.0008 Å |
| c |
15.8408 ± 0.0011 Å |
| α |
74.345 ± 0.002° |
| β |
81.891 ± 0.002° |
| γ |
89.567 ± 0.002° |
| Cell volume |
2137.1 ± 0.2 Å3 |
| Cell temperature |
120 K |
| Ambient diffraction temperature |
120 K |
| Number of distinct elements |
3 |
| Space group number |
2 |
| Hermann-Mauguin space group symbol |
P -1 |
| Hall space group symbol |
-P 1 |
| Residual factor for all reflections |
0.0526 |
| Residual factor for significantly intense reflections |
0.0445 |
| Weighted residual factors for significantly intense reflections |
0.1054 |
| Weighted residual factors for all reflections included in the refinement |
0.1116 |
| Goodness-of-fit parameter for all reflections included in the refinement |
1.036 |
| Diffraction radiation wavelength |
0.71073 Å |
| Diffraction radiation type |
MoKα |
| Has coordinates |
Yes |
| Has disorder |
Yes |
| Has Fobs |
No |
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The link is:
https://www.crystallography.net/7131945.html
