Information card for entry 7132386

Structure parameters

• Formula: C90 H66 B2 F40 Ni P2
• Calculated formula: C90 H66 B2 F40 Ni P2
• Title of publication: Accessing Ni(0) to Ni(IV) <i>via</i> nickel-carbon-phosphorus bond reorganization.
• Authors of publication: Lin, Lirong; Tresp, David S.; Spasyuk, Denis M.; Lalancette, Roger A.; Prokopchuk, Demyan E.
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2024
• Journal volume: 60
• Journal issue: 6
• Pages of publication: 674 - 677
• a: 14.818 ± 0.0003 Å
• b: 16.711 ± 0.0003 Å
• c: 19.124 ± 0.0005 Å
• α: 94.76 ± 0.002°
• β: 90.21 ± 0.002°
• γ: 90.44 ± 0.002°
• Cell volume: 4719.04 ± 0.18 ų
• Cell temperature: 110 K
• Ambient diffraction temperature: 110 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1752
• Residual factor for significantly intense reflections: 0.1558
• Weighted residual factors for significantly intense reflections: 0.3887
• Weighted residual factors for all reflections included in the refinement: 0.4047
• Goodness-of-fit parameter for all reflections included in the refinement: 1.028
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No