Information card for entry 7132388

Structure parameters

• Formula: C93 H21 O36 Si21 U3
• Calculated formula: C84 O36 Si21 U3
• Title of publication: A trinuclear metallasilsesquioxane of uranium(III).
• Authors of publication: Tricoire, Maxime; Jori, Nadir; Fadaei Tirani, Farzaneh; Scopelliti, Rosario; Z Ivković, Ivica; Natrajan, Louise S.; Mazzanti, Marinella
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2023
• Journal volume: 60
• Journal issue: 1
• Pages of publication: 55 - 58
• a: 14.7163 ± 0.0007 Å
• b: 22.3387 ± 0.0009 Å
• c: 24.009 ± 0.0011 Å
• α: 65.307 ± 0.004°
• β: 87.504 ± 0.004°
• γ: 78.555 ± 0.004°
• Cell volume: 7021.6 ± 0.6 ų
• Cell temperature: 140 ± 0.1 K
• Ambient diffraction temperature: 140 ± 0.1 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1968
• Residual factor for significantly intense reflections: 0.1307
• Weighted residual factors for significantly intense reflections: 0.349
• Weighted residual factors for all reflections included in the refinement: 0.3936
• Goodness-of-fit parameter for all reflections included in the refinement: 1.202
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No