Information card for entry 7132449

Structure parameters

• Formula: C28 H36 Cl2 Ge N4
• Calculated formula: C28 H36 Cl2 Ge N4
• SMILES: [Ge](Cl)(Cl)C(=N#N)c1n(cc[n+]1c1c(cccc1C(C)C)C(C)C)c1c(cccc1C(C)C)C(C)C
• Title of publication: Synthesis and isolation of a cyclic bis-vinyl germylene <i>via</i> a diazoolefin adduct of germylene dichloride.
• Authors of publication: Eisner, Teresa; Kostenko, Arseni; J Kiefer, Fiona; Inoue, Shigeyoshi
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2024
• Journal volume: 60
• Journal issue: 5
• Pages of publication: 558 - 561
• a: 9.1689 ± 0.0006 Å
• b: 16.185 ± 0.0009 Å
• c: 22.5667 ± 0.0013 Å
• α: 90°
• β: 94.33 ± 0.003°
• γ: 90°
• Cell volume: 3339.3 ± 0.3 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0646
• Residual factor for significantly intense reflections: 0.0405
• Weighted residual factors for significantly intense reflections: 0.109
• Weighted residual factors for all reflections included in the refinement: 0.1203
• Goodness-of-fit parameter for all reflections included in the refinement: 1.026
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No