Information card for entry 7132535

Structure parameters

• Formula: C76 H70 Cl8 Ga2 N10 O P4
• Calculated formula: C76 H70 Cl8 Ga2 N10 O P4
• Title of publication: Addition and NN bond cleavage of diazo-compounds by phosphino-phosphenium cations.
• Authors of publication: Kim, Hyehwang; Lough, Alan; Qu, Zheng-Wang; Grimme, Stefan; Stephan, Douglas W.
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2024
• Journal volume: 60
• Journal issue: 8
• Pages of publication: 1031 - 1034
• a: 9.9147 ± 0.0007 Å
• b: 18.9028 ± 0.0013 Å
• c: 23.475 ± 0.0017 Å
• α: 68.039 ± 0.003°
• β: 85.656 ± 0.003°
• γ: 76.81 ± 0.003°
• Cell volume: 3972.5 ± 0.5 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0642
• Residual factor for significantly intense reflections: 0.0532
• Weighted residual factors for significantly intense reflections: 0.1339
• Weighted residual factors for all reflections included in the refinement: 0.142
• Goodness-of-fit parameter for all reflections included in the refinement: 1.057
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No