Crystallography Open Database

Information card for entry 7132725

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Coordinates	7132725.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C80 H192 N40 P8 U4
Calculated formula	C80 H192 N40 P8 U4
Title of publication	Temperature induced single-crystal to single-crystal transformation of uranium azide complexes.
Authors of publication	Li, Kai; Rajeshkumar, Thayalan; Zhao, Yue; Wang, Tianwei; Maron, Laurent; Zhu, Congqing
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2024
Journal volume	60
Journal issue	21
Pages of publication	2966 - 2969
a	24.9458 ± 0.0011 Å
b	10.2858 ± 0.0005 Å
c	25.3172 ± 0.0012 Å
α	90°
β	111.158 ± 0.001°
γ	90°
Cell volume	6058.2 ± 0.5 Å³
Cell temperature	193 K
Ambient diffraction temperature	193 K
Number of distinct elements	5
Space group number	13
Hermann-Mauguin space group symbol	P 1 2/n 1
Hall space group symbol	-P 2yac
Residual factor for all reflections	0.0905
Residual factor for significantly intense reflections	0.0491
Weighted residual factors for significantly intense reflections	0.0912
Weighted residual factors for all reflections included in the refinement	0.1071
Goodness-of-fit parameter for all reflections included in the refinement	1.022
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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