Information card for entry 7132729

Structure parameters

• Formula: C20 H48 N10 P2 U
• Calculated formula: C20 H48 N10 P2 U
• SMILES: [U]12(N(CC[N]1(C)C)P(C(C)C)C(C)C)(N(CC[N]2(C)C)P(C(C)C)C(C)C)([N]#N)([N]#N)N=N#N
• Title of publication: Temperature induced single-crystal to single-crystal transformation of uranium azide complexes.
• Authors of publication: Li, Kai; Rajeshkumar, Thayalan; Zhao, Yue; Wang, Tianwei; Maron, Laurent; Zhu, Congqing
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2024
• Journal volume: 60
• Journal issue: 21
• Pages of publication: 2966 - 2969
• a: 24.9421 ± 0.0016 Å
• b: 10.2665 ± 0.0007 Å
• c: 25.3542 ± 0.0019 Å
• α: 90°
• β: 111.169 ± 0.002°
• γ: 90°
• Cell volume: 6054.3 ± 0.7 ų
• Cell temperature: 193 K
• Ambient diffraction temperature: 193 K
• Number of distinct elements: 5
• Space group number: 13
• Hermann-Mauguin space group symbol: P 1 2/n 1
• Hall space group symbol: -P 2yac
• Residual factor for all reflections: 0.1098
• Residual factor for significantly intense reflections: 0.0607
• Weighted residual factors for significantly intense reflections: 0.132
• Weighted residual factors for all reflections included in the refinement: 0.1579
• Goodness-of-fit parameter for all reflections included in the refinement: 1.033
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No